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2 article(s) from Allain, Magali

Tetrathiafulvalene-based azine ligands for anion and metal cation coordination

Awatef Ayadi,
Aziz El Alamy,
Olivier Alévêque,
Magali Allain,
Nabil Zouari,
Mohammed Bouachrine and
Abdelkrim El-Ghayoury

Beilstein J. Org. Chem. 2015, 11, 1379–1391, doi:10.3762/bjoc.11.149

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Scheme 1: Multifunctional TTF-appended azine ligands.

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Scheme 2: Synthetic scheme for TTF-based azine ligands L1 and L2.

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Figure 1: Crystal structure of ligand L1 with atom numbering scheme (top) and a side view of the molecule (bo...

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Figure 2: Partial crystal packing of ligand L1 with formation of head to tail dimers that stack along a-axis ...

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Figure 3: Packing diagram of L1 showing the orientation of the columns of head to tail dimers.

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Figure 4: UV–visible absorption spectra of ligands L1 and L2 (c 2.5 × 10⁻⁵ M in (dichloromethane/acetonitrile...

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Figure 5: HOMO–LUMO Frontier orbitals representation for ligands L1 and L2.

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Figure 6: Cyclic voltammograms of ligands L1 and L2 (2 × 10⁻⁵ M) in CH₂Cl₂/CH₃CN (9:1, v/v) at 100 mV·s⁻¹ on ...

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Figure 7: UV–visible spectral changes of ligand L2 (2 × 10⁻⁵ M in CH₂Cl₂/CH₃CN, 9/1) upon addition of TBAF.

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Figure 8: ¹H NMR spectra of ligand L2 (4·10⁻³ M in DMSO-d₆) upon addition of successive aliquots of TBAF (DMS...

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Figure 9: Crystal structure of complex 3 with atom numbering scheme (top) and a side view of the molecule (bo...

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Figure 10: Pattern of intramolecular and intermolecular contacts in 3. Two molecules are linked by pairs of st...

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Figure 11: Layered structure of complex 3 viewed along the a-axis. The dimers are linked together through hydr...

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Full Research Paper

Published 07 Aug 2015

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Tuning the size of a redox-active tetrathiafulvalene-based self-assembled ring

Sébastien Bivaud,
Sébastien Goeb,
Vincent Croué,
Magali Allain,
Flavia Pop and
Marc Sallé

Beilstein J. Org. Chem. 2015, 11, 966–971, doi:10.3762/bjoc.11.108

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Scheme 1: Synthesis of ligand L1, self-assemblies M₄L₂ and M₆L₃.

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Figure 1: X-ray crystal structures of: (a) ligand L1, (b) self-assembly M₄L₂. For clarity, H atoms and TfO⁻ c...

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Figure 2: ¹H NMR, downfield region (α and β signals correspond respectively to α and β pyridyl protons): (a) ...

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Figure 3: X-ray crystal structure of self-assembly M₆L₃. For clarity, H atoms and TfO⁻ counteranions have bee...

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Figure 4: Geometry (from XRD) around two Pd centers in M₄L₂ (a) and M₆L₃ (b). The exTTF moieties have been cu...

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Figure 5: Cyclic voltammogram of L1 (c = 10⁻³ M, CH₃CN/CH₂Cl₂ (v/v 50/50), 0.1 M n-Bu₄NPF₆, 100 mV·s⁻¹, Pt), M...

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Letter

Published 05 Jun 2015

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